(4-甲基苯基)吗啉-4-基甲酮合成路线 (共 37 条)
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation; SolventTime;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
反应条件
in dichloromethane
T=0 - 20°C; 0.333333 h;
参考文献
Tamaru, Shun-Ichi; Yu, Lianhe; Youngblood, W. Justin; Muthukumaran, Kannan; Taniguchi, Masahiko; Lindsey, Jonathan S.
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 765 - 777
反应条件
tert.-butylhydroperoxide in acetonitrile
T=80°C; 5 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether in toluene
T=105°C; P=3000.3 Torr; 12 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ngiam, Joyce S. Y.; Ghosh, Subhash C.; Chen, Anqi; Seayad, Abdul M.
ACS Catalysis, 2013 , vol. 3, # 6 p. 1406 - 1410
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
24 h; Reflux;
参考文献
Rieke, Reuben D.; Kim, Seung-Hoi
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3478 - 3481
反应条件
potassium carbonate in toluene
T=120°C; 8 h;
参考文献
Dang, Tuan T.; Zhu, Yinghuai; Ghosh, Subhash C.; Chen, Anqi; Chai, Christina L. L.; Seayad, Abdul M.
Chemical Communications, 2012 , vol. 48, # 12 p. 1805 - 1807
反应条件
tert.-butylhydroperoxide; manganese(IV) oxide in water; acetonitrile
T=80°C; 48 h;
参考文献
Vanjari, Rajeshwer; Guntreddi, Tirumaleswararao; Singh, Krishna Nand
Organic Letters, 2013 , vol. 15, # 18 p. 4908 - 4911
反应条件
1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; potassium tert-butylate; palladium diacetate
T=190°C; Heck carbonylation; 0.333333 h; microwave irradiation;
参考文献
Wan, Yiqian; Alterman, Mathias; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 2002 , vol. 67, # 17 p. 6232 - 6235
反应条件
sodium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in water
T=170°C; 0.166667 h; microwave irradiation;
参考文献
Wu, Xiongyu; Larhed, Mats
Organic Letters, 2005 , vol. 7, # 15 p. 3327 - 3329