3-(4-溴苯氧基)-1,2-丙烷二醇合成路线 (共 6 条)
反应条件
osmium(VIII) oxide; N-methyl-2-indolinone; water in acetone; tert-butyl alcohol
T=20°C; Addition; Dihydroxylation;
参考文献
Koelbel, Marius; Beyersdorff, Tom; Tschierske, Carsten; Diele, Siegmar; Kain, Jens
Chemistry - A European Journal, 2000 , vol. 6, # 20 p. 3821 - 3837
反应条件
ethanol; sodium ethanolate
参考文献
Roushdi; Ibrahim
Acta Pharmaceutica Internationalia, 1950 , vol. 1, p. 311,316
反应条件
1: BBr3 / CH2Cl2 / 20 °C
2: K2CO3 / acetonitrile / Heating
3: OsO4; NMMNO / acetone / 20 °C
View Scheme
参考文献
Koelbel; Beyersdorff; Xiao Hong Cheng; Tschierske; Kain; Diele
Journal of the American Chemical Society, 2001 , vol. 123, # 28 p. 6809 - 6818
反应条件
1: K2CO3 / acetonitrile / Heating
2: OsO4; NMMNO / acetone / 20 °C
View Scheme
参考文献
Koelbel; Beyersdorff; Xiao Hong Cheng; Tschierske; Kain; Diele
Journal of the American Chemical Society, 2001 , vol. 123, # 28 p. 6809 - 6818
反应条件
triethylamine in ethanol
Heating;
参考文献
Bredikhina; Savel'ev; Bredikhin
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 2 p. 213 - 219
反应条件
man leitet durch die mit Wasser versetzte Reaktionsfluessigkeit Brom;
参考文献
Hantzsch; Vock
Chemische Berichte, 1903 , vol. 36, p. 2062