反应条件
tetrakis(triphenylphosphine) palladium(0) in diethyl ether addn. of Ph3SnCl in ether to suspn. of LiAlH4 in ether (-10°C), heating to 20°C (in 30 min, stirring 3 h), addn. of water, sepn. of org. layer, extn. of residue (ether), drying of org. phases, evapn., addn. of toluene and catalyst, pptn.; filtration off, washing (toluene, drying (air), extn. (CHCl3), chromy. (silica gel), removal of solvent;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 1044 - 1049
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 5 p. 1137 - 1142
