hydrogenchloride in tert-butyl methyl ether; water T=20°C; 18 h;

water und Erwaermen des Reaktionsprodukts mit wss. Salzsaeure;

1: ammonium acetate; acetic acid / 12 h / 100 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 80 °C 3: hydrogenchloride / water / 1 h / 60 °C 4: hydrogenchloride / water; tert-butyl methyl ether / 18 h / 20 °C View Scheme

1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 80 °C 2: hydrogenchloride / water / 1 h / 60 °C 3: hydrogenchloride / water; tert-butyl methyl ether / 18 h / 20 °C View Scheme

1: hydrogenchloride / water / 1 h / 60 °C 2: hydrogenchloride / water; tert-butyl methyl ether / 18 h / 20 °C View Scheme

sodium hydrogencarbonate in water T=20°C; 0.5 h;