(3-甲基苄基)膦酸二乙酯合成路线 （共 9 条）
参考文献
US2012/22293 A1, ;
Page/Page column 10 ;
反应条件
iodine in methanol 1.5 h; Heating;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1455 - 1460
反应条件
1: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 20-60 min, 2.) THF, hexane, -78 deg C, 1 h 2: 12 percent / iodine / 1.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1455 - 1460
反应条件
1: 1.) butyllithium / 1.) THF, hexane, -78 deg C, 20-60 min, 2.) THF, hexane, -78 deg C, 1 h 2: 12 percent / iodine / 1.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1455 - 1460
反应条件
iodine 1.5 h; Heating;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1455 - 1460
参考文献
Tetrahedron, , vol. 55, # 9 p. 2671 - 2686
反应条件
sodium hydride
1.) DMSO; Yield given. Multistep reaction;
参考文献
Tominaga, Yoshinori; Pratap, Ram; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 871 - 877
反应条件
n-butyllithium
1) THF, 15 min, RT; 2) 15 min, RT; Yield given. Multistep reaction;
参考文献
Porskamp, Pascal A. T. W.; Lammerink, Ben H. M.; Zwanenburg, Binne
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 263 - 268
反应条件
1: 1) n-BuLi / 1) THF, 15 min, RT; 2) 15 min, RT
View Scheme
参考文献
Porskamp, Pascal A. T. W.; Lammerink, Ben H. M.; Zwanenburg, Binne
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 263 - 268
