(4-氟苄基)膦酸二乙酯合成路线 （共 12 条）
反应条件
1: 1.) n-BuLi, HMDS, 2.) Cl3C-CCl3 / 1.) hexane, THF, -78 deg C -> 20 deg C; 20 deg C, 15 min, 2.) THF, -78 deg C, 15 min; -78 deg C -> 0 deg C
2: EtOLi / ethanol / 0.25 h / 0 °C
View Scheme
参考文献
Iorga, Bogdan; Eymery, Frederic; Savignac, Philippe
Tetrahedron Letters, 1998 , vol. 39, # 22 p. 3693 - 3696
反应条件
hydrogenchloride
Heating;
参考文献
Montoneri, E.; Savarino, P.; Viscardi, G.; Gallazzi, M. C.
Phosphorus, Sulfur and Silicon and the Related Elements, 1994 , vol. 86, # 1-4 p. 145 - 156
