2-[2-(四氢呋喃-2-基)乙基]-1,6-二氧杂螺[4.4]壬烷合成路线 （共 7 条）
反应条件
ethanol; copper oxide-chromium oxide
T=110 - 135°C; P=77228.3 - 91938.4 Torr; Hydrogenation.anschliessendes Hydrieren an Raney-Nickel;
参考文献
Alexander et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 5506,5507
Journal of the American Chemical Society, 1951 , vol. 73, p. 2725,2726
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=140°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=120°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
1: T=140°C; 5 h;
2: With hydrogen in isopropyl alcohol
T=80°C; P=30003 Torr; 10 h;
参考文献
Xu, Wenjie; Liu, Xiaohui; Ren, Jiawen; Zhang, Peng; Wang, Yanqin; Guo, Yanglong; Guo, Yun; Lu, Guanzhong
Catalysis Communications, 2010 , vol. 11, # 8 p. 721 - 726
反应条件
nickel
Hydrogenation;
参考文献
Alexander et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 5506,5507
Journal of the American Chemical Society, 1951 , vol. 73, p. 2725,2726
反应条件
hydrogen; Al-Ni-Ti alloy in ethanol
T=50°C; P=760 Torr; 5 h; other solvents,other temperatures, other pressures; MechanismRate constantProduct distribution;
参考文献
Mat'yakubov, R.; Mamatov, Yu. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 7 p. 651 - 655
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , # 7 p. 889 - 893
反应条件
T=120°C; P=73550.8 Torr; Hydrogenation;
参考文献
Balandin; Ponomarew
Doklady Akademii Nauk SSSR, 1955 , vol. 100, p. 917,919
Chem.Abstr., 1956 , p. 1746
