(2-氯苯基)-吗啉-4-甲酮合成路线 （共 8 条）
反应条件
tetrahydroxydiboron; chloro(2-dicyclohexylphosphino-2',4',6'-triisoporpyl-1,1'-biphenyl)[2-(2'-amino-1,1'-biphenyl)] palladium (II); potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in ethanol T=80°C; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Kennedy, Steven M.; Dreher, Spencer D.; Tudge, Matthew T.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11667 - 11673
反应条件
cesium fluoride; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran
T=80°C; 16 h;
参考文献
Lysen, Morten; Kelleher, Susan; Begtrup, Mikael; Kristensen, Jesper Langgaard
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5342 - 5343
参考文献
Kuliev; Kurbanov; Mamedov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 1 pt 2 p. 139 - 142
反应条件
1: tert.-butylhydroperoxide; copper (II) acetate monohydrate / water; acetonitrile / 0.67 h / |Inert atmosphere; |Reflux
2: water; acetonitrile / 0.5 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Pilo, Monica; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8241 - 8246
反应条件
in water; acetonitrile
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Pilo, Monica; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8241 - 8246
反应条件
1: PCl5 / 1,2-dichloro-ethane / 3 h / 83 °C
2: 80.2 percent / benzene / 1 h
View Scheme
参考文献
Kuliev; Kurbanov; Mamedov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 1 pt 2 p. 139 - 142
反应条件
tetraphosphorus decasulfide in benzene
3 h;
参考文献
Kuliev; Kurbanov; Mamedov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 1 pt 2 p. 139 - 142
反应条件
tetrahydroxydiboron; chloro(2-dicyclohexylphosphino-2',4',6'-triisoporpyl-1,1'-biphenyl)[2-(2'-amino-1,1'-biphenyl)] palladium (II); potassium acetate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in ethanol
T=80°C; 4 h; Inert atmosphere;
参考文献
Molander, Gary A.; Trice, Sarah L. J.; Kennedy, Steven M.; Dreher, Spencer D.; Tudge, Matthew T.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11667 - 11673
