in tetrahydrofuran under N2; addn. of α-imino ketone to stirred suspn. of Fe2(CO)9 in THF, stirring for 2 h at room temp.; bubbling air through soln. for 5 min, evapn., column chromy. (SiO2, pentane for Fe3(CO)12, 7:1 pentane/Et2O for Fe2(CO)6 complex), crystn. frompentane at -60°C (Fe2(CO)6 complex);
参考文献
Siebenlist, Ron; Fruehauf, Hans-Werner; Vrieze, Kees; Smeets, Wilberth J. J.; Spek, Anthony L.
European Journal of Inorganic Chemistry, 2000 , # 5 p. 907 - 919
