in further solvent(s)
byproducts: H2, CH4, C2H6; a suspension of 9-BBN and Fe3(CO)12 in nonane was slowly heated to above 130°C (bath temp.) under an inert gas atm.; stirring for about 0.5 h; further products and byproducts; mechanism discussed;; distn. under vac.; mixt. of 9-alkyl-9-BBN obtained, detected by GC/MS;;
in further solvent(s)
byproducts: H2, CH4, C2H6; a suspension of 9-BBN and Fe(CO)5 in nonane was slowly heated to about 140°C (bath temp.) under an inert gas atm.; stirring for about 0.5 h; further products and byproducts; mechanism discussed;; distn. under vac.; mixt. of 9-alkyl-9-BBN obtained, detected by GC/MS;;
in further solvent(s)
byproducts: H2, CH4, C2H6; a suspension of 9-BBN and Fe2(CO)9 in nonane was slowly heated to above140°C (bath temp.) under an inert gas atm.; stirring for about 0.5 h; further products and byproducts; mechanism discussed;; distn. under vac.; mixt. of 9-alkyl-9-BBN obtained, detected by GC/MS;;
in further solvent(s)
byproducts: H2, CH4, C2H6; a suspension of 9-BBN and Co2(CO)8 in nonane was slowly heated to above90°C (bath temp.) under an inert gas atm.; stirring for about 0.5 h; further products and byproducts; mechanism discussed;; distn. under vac.; mixt. of 9-alkyl-9-BBN obtained, detected by GC/MS;;