2-(2-甲酰基苯基)乙酸甲酯合成路线 （共 12 条）
反应条件
toluene-4-sulfonic acid in methanol; diethyl ether
反应条件
1: With ammonia; triethylamine T=-33°C; 2: With CuSO4‵5H2O in tetrahydrofuran; water 2 h; Reflux;
参考文献
Kowalkowska, Anna; Jonczyk, Andrzej
Synthetic Communications, 2011 , vol. 41, # 22 p. 3308 - 3317
反应条件
toluene-4-sulfonic acid 12 h; Ambient temperature;
参考文献
Akbutina; Davydova; Zarudii; Sagitdinov; Miftakhov
Pharmaceutical Chemistry Journal, 1998 , vol. 32, # 5 p. 255 - 257
反应条件
1: With triethylamine in dichloromethane T=20°C; 2 h; 2: With CuSO4‵5H2O in tetrahydrofuran; water 2 h; Reflux;
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
反应条件
CuSO4‵5H2O in tetrahydrofuran; water 2 h; Reflux;
参考文献
Kowalkowska, Anna; Jonczyk, Andrzej
Synthetic Communications, 2011 , vol. 41, # 22 p. 3308 - 3317
反应条件
1: dichloromethane / 20 °C 2: ammonia / -33 °C 3: CuSO4‵5H2O / tetrahydrofuran; water / 2 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
反应条件
1: dichloromethane / Cooling 2: triethylamine / dichloromethane / 2 h / 20 °C 3: CuSO4‵5H2O / tetrahydrofuran; water / 2 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
反应条件
2: ammonia / -33 °C 3: CuSO4‵5H2O / tetrahydrofuran; water / 2 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
反应条件
1: tetrabutylammomium bromide; potassium carbonate / acetonitrile / 10.17 h / 65 - 70 °C 2: dichloromethane / Cooling 3: triethylamine / dichloromethane / 2 h / 20 °C 4: CuSO4‵5H2O / tetrahydrofuran; water / 2 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
反应条件
1: triethylamine / dichloromethane / 2 h / 20 °C 2: CuSO4‵5H2O / tetrahydrofuran; water / 2 h / Reflux View Scheme
参考文献
Synthetic Communications, , vol. 41, # 22 p. 3308 - 3317
