[(3,4-二氯苯基)甲基]膦酸二乙酯合成路线 （共 4 条）
反应条件
T=80°C; 1 h; Heating / reflux;
参考文献
Gong, Leyi
Patent: US2004/176416 A1, 2004 ;
Location in patent: Page/Page column 10 ;
US 20040176416 A1
反应条件
T=120°C; Inert atmosphere;
参考文献
BAYLOR COLLEGE OF MEDICINE; SONG, Yongcheng
Patent: WO2011/46920 A1, 2011 ;
Location in patent: Page/Page column 89-90 ;
反应条件
1: sodium tetrahydroborate; methanol / 1 h / 0 - 20 °C
2: thionyl chloride / dichloromethane / 3 h / 0 - 20 °C
3: 120 °C / Inert atmosphere
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参考文献
BAYLOR COLLEGE OF MEDICINE; SONG, Yongcheng
Patent: WO2011/46920 A1, 2011 ;
反应条件
1: thionyl chloride / dichloromethane / 3 h / 0 - 20 °C
2: 120 °C / Inert atmosphere
View Scheme
参考文献
BAYLOR COLLEGE OF MEDICINE; SONG, Yongcheng
Patent: WO2011/46920 A1, 2011 ;
