1: 72 percent / tetrabutylammonium bromide / benzene / 3 h / Heating 2: immobilized baker's yeast, glucose / H2O / 72 h / 35 °C 3: 56 percent / Ba(OH)2 / H2O; ethanol / 3 h / 85 °C View Scheme
参考文献
Sakai, Takashi; Wada, Kou; Murakami, Takahiko; Kohra, Kiichiro; Imajo, Norihisa; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 3 p. 631 - 638
1: in tetrahydrofuran; diethyl ether
T=0 - 20°C; 3 h;
2: With hydrogenchloride in tetrahydrofuran; diethyl ether; water
参考文献
THE GOVERNING COUNCIL OF THE UNIVERSITY OF TORONTO; SEFEROS, Dwight; JAHNKE, Ashlee
Patent: WO2014/67016 A1, 2014 ;
Location in patent: Page/Page column 10; 11 ;
1: With trichloroisocyanuric acid; water in acetone
T=20°C; 1 h;
2: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; trichloroisocyanuric acid in dichloromethane
T=20°C; 3 h; Further stages.;
参考文献
Berkessel, Albrecht; Rollmann, Claudia; Chamouleau, Francoise; Labs, Stefanie; May, Oliver; Groeger, Harald
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 17-18 p. 2697 - 2704
aluminium trichloride in neat (no solvent)
T=25°C;
参考文献
Doyle, Michael P.; Buhro, William E.; Davidson, James G.; Elliott, Robert C.; Hoekstra, James W.; Oppenhuizen, Mark
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3657 - 3664
