N-(1-甲基-2-丙炔基)苄胺合成路线 （共 4 条）
反应条件
1: benzyl(1-methyl-prop-2-ynyl)amine With hydrogenchloride in diethyl ether 0.0833333 h; Inert atmosphere; 2: oxalyl dichloride in ethylene glycol dimethyl ether T=170°C; 0.166667 h; Microwave irradiationAutoclave;
参考文献
Gising, Johan; Oertqvist, Pernilla; Sandstroem, Anja; Larhed, Mats
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 13 p. 2809 - 2815
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,4-dioxane
T=10 - 20°C; Substitution; 3 h;
参考文献
Wipf, Peter; Hopkins, Corey R.
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6881 - 6887
反应条件
in ethylene glycol dimethyl ether
T=60°C; Strecker reaction; 0.166667 h; AutoclaveMicrowave irradiation;
参考文献
Gising, Johan; Oertqvist, Pernilla; Sandstroem, Anja; Larhed, Mats
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 13 p. 2809 - 2815
反应条件
nitrogen; copper(l) chloride
参考文献
I.G.Farbenind.
Patent: DE730850 , 1937 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Gen.Aniline and Film Corp.
Patent: US2268129 , 1938 ;
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Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
