acetic acid in N,N-dimethyl-formamide
T=80 - 140°C; 10 h; no temperature effects (80 - 140 deg C); regioselective alkylation (5-nitro-isomer); Product distributionMechanism;
参考文献
Rao, A. K. S. Bhujanga; Rao, C. Gundu; Singh, B. B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2399 - 2402
1: 3-(p-hydroxyphenyl)-3-methyl-2-butanone With phenoxide resin IRA-400 in 1,2-dichloro-benzene
2: diethyl sulphate in tetrahydrofuran
0.05 h; microwave irradiation; Further stages.;
参考文献
Gopalakrishnan, Geetha; Kasinath, Viswanathan; Singh, N. D. Pradeep
Organic Letters, 2002 , vol. 4, # 5 p. 781 - 782