反应条件
1: phenyllithium With DABCO-bis(sulfur dioxide) in 1,4-dioxane T=20°C; 2 h; Inert atmosphereSchlenk technique; 2: 1-(iodo)-4-methylbenzene; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene With palladium diacetate; caesium carbonate T=70°C; 16 h; Inert atmosphereSchlenk technique; Reagent/catalystTemperature;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 48 p. 12679 - 12683
Angew. Chem., , vol. 125, # 48 p. 12911 - 12915,5
