反应条件
1: 76 percent / CH2Cl2 / 48 h / Ambient temperature 2: 1) BuLi / 1) THF, hexane, -65 deg C, 20 min, 2) THF, -80 deg C, 2h 3: 1) KOCl / 1) dioxane, 2) THF 4: 1) 0.10M HCl, 2) 2.0M NaOH / 1) CH3CN, RT, 18h, 2) 70 deg C, 15 min View Scheme
参考文献
Tetrahedron, , vol. 47, # 3 p. 497 - 506
