5-(4-甲苯基)异噁唑-3-甲醛合成路线 （共 6 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 5 h;
参考文献
Synthesis, , # 15 p. 2325 - 2330
反应条件
formaldehyd; sulfuric acid; water 6 h; Reflux;
参考文献
Potkin; Petkevich; Kletskov; Dikusar; Zubenko; Zhukovskaya; Kazbanov; Pashkevich
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1523 - 1533
Zh. Org. Khim., 2013 , vol. 49, # 10 p. 1543 - 1553,11
反应条件
1: NH2OH*HCl / ethanol / 1 h / Heating 2: LiAlH4 / diethyl ether / 0.5 h / 40 °C 3: PCC / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2325 - 2330
反应条件
1: LiAlH4 / diethyl ether / 0.5 h / 40 °C 2: PCC / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2325 - 2330
反应条件
1.1: NaH / toluene / 45 - 50 °C 1.2: toluene / 1.5 h / Heating 2.1: NH2OH*HCl / ethanol / 1 h / Heating 3.1: LiAlH4 / diethyl ether / 0.5 h / 40 °C 4.1: PCC / CH2Cl2 / 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 15 p. 2325 - 2330
反应条件
sodium tetrahydroborate; isopropyl alcohol 4 h;
参考文献
Potkin; Petkevich; Kletskov; Dikusar; Zubenko; Zhukovskaya; Kazbanov; Pashkevich
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1523 - 1533
Zh. Org. Khim., 2013 , vol. 49, # 10 p. 1543 - 1553,11
