(三甲基硅基)甲基三氟甲烷磺酸酯合成路线 (共 16 条)
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium
1.) THF, -78 deg C; 2.) room temp.; Yield given. Multistep reaction;
参考文献
Chiu, Sai Keung; Peterson, Paul E.
Tetrahedron Letters, 1980 , vol. 21, p. 4047 - 4050
反应条件
n-butyllithium in tetrahydrofuran; hexane
-78 deg C then room temp.;
参考文献
Gallagher, Timothy; Magnus, Phillip
Tetrahedron, 1981 , vol. 37, # 23 p. 3889 - 3898
反应条件
in ethylene glycol dimethyl ether
12 h; Ambient temperature;
参考文献
Aono, Masahiro; Terao, Yoshiyasu; Achiwa, Kazuo
Chemistry Letters, 1987 , p. 1851 - 1852
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
T=20°C; Alkylation;
参考文献
Bell, Stephanie E. V.; Brown, Roger F.C.; Eastwood, Frank W.; Horvath, Julianna M.
Australian Journal of Chemistry, 2000 , vol. 53, # 3 p. 183 - 190
反应条件
benzaldehyde; cesium fluoride
1.) CH3CN, RT, 2 h, 2.) CH3CN, 1 h; Yield given. Multistep reaction;
参考文献
Cohen, Theodore; Kosarych, Zenyk; Suzuki, Kunio; Yu, Lin-Chen
Journal of Organic Chemistry, 1985 , vol. 50, # 16 p. 2965 - 2968
反应条件
Yield given. Multistep reaction;
参考文献
Majetich; Leigh
Tetrahedron Letters, 1991 , vol. 32, # 5 p. 609 - 610