4-乙酰基-4-溴丁酸甲酯合成路线 （共 3 条）
反应条件
bromine in diethyl ether
T=0 - 20°C;
参考文献
Toth, Florian; Kalaus, Gyoergy; Greiner, Istvan; Kajtar-Peredy, Maria; Goemoery, Agnes; Hazai, Laszlo; Szantay, Csaba
Tetrahedron, 2006 , vol. 62, # 51 p. 12011 - 12016
反应条件
1: 86 percent / sodium borohydride / methanol / 0 - 20 °C
2: 78 percent / imidazole / CH2Cl2 / 24 h / Heating
3: 72 percent / diisobutyl aluminum hydride / CH2Cl2; hexane / 0.75 h / -60 °C
View Scheme
参考文献
Toth, Florian; Kalaus, Gyoergy; Greiner, Istvan; Kajtar-Peredy, Maria; Goemoery, Agnes; Hazai, Laszlo; Szantay, Csaba
Tetrahedron, 2006 , vol. 62, # 51 p. 12011 - 12016
反应条件
sodium tetrahydroborate in methanol
T=0 - 20°C;
参考文献
Toth, Florian; Kalaus, Gyoergy; Greiner, Istvan; Kajtar-Peredy, Maria; Goemoery, Agnes; Hazai, Laszlo; Szantay, Csaba
Tetrahedron, 2006 , vol. 62, # 51 p. 12011 - 12016
