反应条件
in diethyl ether
dropwise addn. of stannane in Et2O to LiCH2PMe2 in Et2O at -78°Cwith stirring, warming to room temp., stirring for 12 h; evapn. of solvent in vacuo, redissolution in pentane, filtn., washing residue with pentane (two times), evapn. of solvent in vacuo, fractionating in vacuo, elem. anal.;
参考文献
Karsch, Hans H.; Appelt, Armin
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1983 , vol. 38, # 11 p. 1399 - 1405
