3,4-二甲氧基联苯-4-甲醛合成路线 （共 3 条）
反应条件
18-crown-6 ether; 10 Pd/C; potassium carbonate in methanol; water
T=45°C; Suzuki-Miyaura Coupling; 0.5 h;
参考文献
Chu, Wenyi; Li, Xinmin; Hou, Yanjun; Wang, Hua; Li, Hongyu; Yuan, Xiaobin; Sun, Zhizhong
Applied Organometallic Chemistry, 2012 , vol. 26, # 9 p. 478 - 482
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Rosen, Brad M.; Wilson, Daniela A.; Wilson, Christopher J.; Peterca, Mihai; Won, Betty C.; Huang, Chenghong; Lipski, Linda R.; Zeng, Xiangbing; Ungar, Goran; Heiney, Paul A.; Percec, Virgil
Journal of the American Chemical Society, 2009 , vol. 131, # 47 p. 17500 - 17521
反应条件
1: sodium hydride / tetrahydrofuran; mineral oil / |Inert atmosphere; |Reflux
2: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0 °C
3: trifluoroacetic acid / dichloromethane; methanol / 20 °C
4: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0 - 20 °C
5: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 3 h / 20 °C
View Scheme
参考文献
Rankin, Gregory M.; Maxwell-Cameron, Isobel; Painter, Gavin F.; Larsen, David S.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5264 - 5272
