1: With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran; cyclohexane T=-75°C; 2 h; 2: With bromine in tetrahydrofuran; cyclohexane T=-75°C; Further stages.;
参考文献
Castagnetti, Eva; Schlosser, Manfred
European Journal of Organic Chemistry, 2001 , # 4 p. 691 - 695
bromine; iron(III) chloride in nitromethane T=25°C; 1 h; investigation of the bromination reaction; relative reactivity data compared to benzene; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 3708
1: With n-butyllithium in tetrahydrofuran T=-78°C; 0.75 h; 2: With tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; 16 h; 3: With hydrogenchloride; sodium hydroxide; water more than 3 stages;
参考文献
MERCK and CO., INC.
Patent: WO2005/97136 A1, 2005 ;
Location in patent: Page/Page column 30 ;
WO 2005/097136 A1
