4-羟基邻苯二甲酸二乙酯合成路线 （共 12 条）
反应条件
1: concentrated KOH-solution 2: 200 °C View Scheme
参考文献
Baeyer
Chemische Berichte, 1877 , vol. 10, p. 1079
参考文献
Chemische Berichte, , vol. 10, p. 1079
Chemische Berichte, , vol. 11, p. 1191
Justus Liebigs Annalen der Chemie, , vol. 208, p. 236
反应条件
sulfuric acid
Heating;
参考文献
Illumina Cambridge Limited; Romanov, Nikolai Nikolaevich; Liu, Xiaohai
Patent: US8754244 B1, 2014 ;
Location in patent: Page/Page column 25; 26 ;
反应条件
1: Me3SiOTf / various solvent(s)
2: 1.) NaOEt; 2.) I2 / ethanol / Ambient temperature
View Scheme
参考文献
Hegde, Shridhar G.; Kassim, Amude M.; Ingrum, April I.
Tetrahedron Letters, 1995 , vol. 36, # 46 p. 8395 - 8398
反应条件
1: toluene / Heating
2: Me3SiOTf / various solvent(s)
3: 1.) NaOEt; 2.) I2 / ethanol / Ambient temperature
View Scheme
参考文献
Hegde, Shridhar G.; Kassim, Amude M.; Ingrum, April I.
Tetrahedron Letters, 1995 , vol. 36, # 46 p. 8395 - 8398
反应条件
iodine; sodium ethanolate in ethanol
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hegde, Shridhar G.; Kassim, Amude M.; Ingrum, April I.
Tetrahedron Letters, 1995 , vol. 36, # 46 p. 8395 - 8398
反应条件
1: benzene / 48 h / Heating
2: benzene / Heating
View Scheme
参考文献
Buckle, Ronald N.; Liu, Pei-Ying; Roberts, Evan W. D.; Burnell, D. Jean
Tetrahedron, 1999 , vol. 55, # 38 p. 11455 - 11464
反应条件
in benzene
Elimination; retro-Diels-Alder reaction; Heating;
参考文献
Buckle, Ronald N.; Liu, Pei-Ying; Roberts, Evan W. D.; Burnell, D. Jean
Tetrahedron, 1999 , vol. 55, # 38 p. 11455 - 11464
反应条件
in benzene
Elimination; retro-Diels-Alder reaction; Heating;
参考文献
Buckle, Ronald N.; Liu, Pei-Ying; Roberts, Evan W. D.; Burnell, D. Jean
Tetrahedron, 1999 , vol. 55, # 38 p. 11455 - 11464
反应条件
in benzene
Elimination; retro-Diels-Alder reaction; Heating;
参考文献
Buckle, Ronald N.; Liu, Pei-Ying; Roberts, Evan W. D.; Burnell, D. Jean
Tetrahedron, 1999 , vol. 55, # 38 p. 11455 - 11464
