三(N,N-四亚甲基)磷酰胺合成路线 (共 4 条)
反应条件
in tetrahydrofuran; dichloromethane T=20°C; 18 h;
参考文献
US2006/30583 A1, ;
Page/Page column 132-133 ;
US 20060030583 A1
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane 0.5 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 59, # 9 p. 2437 - 2446
反应条件
KPF6; phosphorus oxytribromide 1.) CH3CN, r.t., 30 min; Yield given. Multistep reaction;
参考文献
Coste, Jacques; Frerot, Eric; Jouin, Patrick
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2437 - 2446
反应条件
hexafluorophosphate; trichlorophosphate Multistep reaction;
参考文献
Coste, J.; Le-Nguyen, D.; Castro, B.
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 205 - 208