[(3E)-5,5,5-三氟-3-戊烯-1-基]苯合成路线 （共 2 条）
反应条件
[bis(acetoxy)iodo]benzene; tri-n-butyl-tin hydride; sodium acetate; silver nitrate in 1-methyl-pyrrolidin-2-one
T=20°C; 6 h; Inert atmosphere; Reagent/catalyst; Overall yield = 36 percentSpectr.;
参考文献
Wu, Xinyue; Chu, Lingling; Qing, Feng-Ling
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2198 - 2202
Angew. Chem., 2013 , vol. 125, # 8 p. 2254 - 2258,5
反应条件
[bis(acetoxy)iodo]benzene; sodium acetate; silver trifluoromethanesulfonate in 1-methyl-pyrrolidin-2-one
T=20°C; 6 h; Inert atmosphere; Reagent/catalyst; Overall yield = 64 percentSpectr.;
参考文献
Wu, Xinyue; Chu, Lingling; Qing, Feng-Ling
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2198 - 2202
Angew. Chem., 2013 , vol. 125, # 8 p. 2254 - 2258,5
