Inhoffen Lythgoe diol合成路线 (共 42 条)
反应条件
Multi-step reaction with 2 steps 1: 99 percent / pyridine; DMAP / 0 °C2: 95 percent / KOH / ethanol; benzene
参考文献
Fall, Yagamare; Barreiro, Candida; Fernandez, Carlos; Mourino, Antonio Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1433 - 1436
反应条件
Multi-step reaction with 2 steps 1.1: imidazole / dimethylformamide / 48 h / 60 °C1.2: 96 percent / HCl / tetrahydrofuran / 1 h / 20 °C2.1: 1.79 g / (diacetoxyiodo)benzene; 2,2,6,6-tetramethylpiperidinooxyl radical / CH2Cl2 / 5 h
参考文献
Moman, Edelmiro; Nicoletti, Daniel; Mourino, Antonio Organic Letters, 2006 , vol. 8, # 6 p. 1249 - 1251