4,4'-苯亚甲基二吗啉合成路线 （共 23 条）
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane
T=20°C; Condensation; 0.5 h;
参考文献
Malhiac, Catherine; Combret, Jean-Claude; Boussad, Kamal; Klein, Jean-Louis
Phosphorus, Sulfur and Silicon and Related Elements, 1996 , vol. 113, # 1-4 p. 299 - 301
反应条件
in dichloromethane
1 h; Ambient temperature;
参考文献
Anders, Ernst; Tropsch, Juergen G.; Katrizky, Alan R.; Rasala, Danuta; Eynde Vanden, Jean-Jacques
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4808 - 4812
反应条件
pentacarbonyliron(0) in N,N-dimethyl-formamide
T=140°C; 2 h; various reaction conditions; Product distributionMechanism;
参考文献
Terent'ev, A. B.; Makaeva, R. M.; Musavirov, R. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 10 p. 2153 - 2155
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 10 p. 2351 - 2353
反应条件
n-butyllithium; sulfur
1. benzene, hexane, r.t., 2. 50 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Okuma, Kentaro; Komiya, Yasuo; Ohta, Hiroshi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2402 - 2406
参考文献
Stewart; Hauser
Journal of the American Chemical Society, 1955 , vol. 77, p. 1098,1100
反应条件
1: 79 percent / 3.5 h / 60 °C
2: 96 percent / 2 h / 50 °C
View Scheme
参考文献
Nikogosyan, L. L.; Nersesyan, K. A.; Satina, T. Ya.; Panosyan, G. A.; Mirzoyan, R. G.; Indzhikyan, M. G.,
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 12.1 p. 2716 - 2721,2434 - 2438
反应条件
copper(l) iodide in acetonitrile
0.5 h; Heating;
参考文献
Komissarov, V. N.; Ukhin, L. Yu.; Orlova, Zh. I.; Tokarskaya, O. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1198 - 1199
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1325 - 1326
反应条件
hydrogenchloride in chloroform
1 h; Ambient temperature;
参考文献
Le Floc'h,Y. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1969 , vol. 268, p. 1718 - 1720
反应条件
hydrogenchloride in chloroform
1 h; Ambient temperature;
参考文献
Le Floc'h,Y. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1969 , vol. 268, p. 1718 - 1720
参考文献
Le Floc'h,Y. et al.
Bulletin de la Societe Chimique de France, 1979 , vol. <II>, p. 409 - 414
