1: (n-propyl)-triphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane T=0 - 20°C; Inert atmosphere; 2: tetrahydropyranyl alcohol in tetrahydrofuran; hexane; toluene 1 h; RefluxInert atmosphere; optical yield given as percent de;
参考文献
Bourgeois, Joffre; Dion, Isabelle; Cebrowski, Pamela H.; Loiseau, Francis; Bedard, Anne-Catherine; Beauchemin, Andre M.
Journal of the American Chemical Society, 2009 , vol. 131, p. 874 - 875