反应条件
1: With IrH5(P-i-Pr3)2; 3,3-dimethylbut-1-ene
T=150°C; 12 h; Inert atmosphere;
2: With Schwartz's reagent in tetrahydrofuran
T=40°C; 24 h; Inert atmosphere;
3: With iodine in tetrahydrofuran
T=25°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Kuninobu, Yoichiro; Ureshino, Tomonari; Yamamoto, Shun-Ichi; Takai, Kazuhiko
Chemical Communications, 2010 , vol. 46, # 29 p. 5310 - 5312