1: With ammonia; sodium t-butanolate; [(CyPF-tBu)PdCl2] in ethylene glycol dimethyl ether T=90°C; P=4137.29 - 10343.2 Torr; 20 h; 2: With hydrogenchloride in ethylene glycol dimethyl ether; water 3: With sodium hydrogencarbonate in ethylene glycol dimethyl ether; water Product distribution / selectivity;
参考文献
YALE UNIVERSITY
Patent: WO2007/109365 A2, 2007 ;
Location in patent: Page/Page column 44; 45; 47 ;
O-(2,4-dinitro-phenyl)-hydroxylamine in toluene T=50°C; 48 h; Inert atmosphere;
参考文献
Zhu, Chen; Li, Gongqiang; Ess, Daniel H.; Falck, John R.; Kuerti, Laszlo
Journal of the American Chemical Society, 2012 , vol. 134, # 44 p. 18253 - 18256
