1: With [{(η5-C5Me5)IrCl}2(μ-Cl)2]; water in dichloromethane T=20°C; 24 h; Schlenk techniqueInert atmosphere; 2: With hydrogenchloride; water in acetonitrile-D3 T=20°C; 24 h; Schlenk techniqueInert atmosphereIrradiation;
参考文献
Journal of Organometallic Chemistry, , vol. 724, p. 275 - 280
1: Li with 2percent Na / tetrahydrofuran / 0.17 h / 15 - 18 °C / Irradiation 2: n-Butyl-litthium / efect of solvents, amids and metellating agents were studied. View Scheme
