4-(三异丙基硅烷基氧基)苯基基硼酸合成路线 （共 2 条）
反应条件
pyridine; copper diacetate; triethylamine; 4 A molecular sieve in dichloromethane
T=20°C;
参考文献
Hart, Matthew E.; Suchland, Katherine L.; Miyakawa, Motonori; Bunzow, James R.; Grandy, David K.; Scanlan, Thomas S.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 3 p. 1101 - 1112
反应条件
1: 40 percent / Cu(OAc)2; Et3N; pyridine / 4 Angstroem molecular sieves / CH2Cl2 / 20 °C
2: 86 percent / TBAF / tetrahydrofuran / 0 °C
3: 100 percent / HCl / ethyl acetate / 20 °C
View Scheme
参考文献
Hart, Matthew E.; Suchland, Katherine L.; Miyakawa, Motonori; Bunzow, James R.; Grandy, David K.; Scanlan, Thomas S.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 3 p. 1101 - 1112
