N6-苯甲酰基-5'-O-(4,4'-二甲氧基三苯基)-2'-脱氧腺苷合成路线 (共 17 条)
参考文献
Tetrahedron Letters, , vol. 33, # 48 p. 7319 - 7323
反应条件
pivaloyl chloride; ethylene glycol T=0°C; Hydrolysis; 0.333333 h;
参考文献
Tetrahedron Letters, , vol. 40, # 35 p. 6477 - 6480
反应条件
1: pyridine / 1 h / 20 °C 2: NaOH / pyridine; ethanol; H2O / 0.25 h 3: 1.) pyridine, 0 deg C, 16 h, 2.) pyridine, CH3OH, 20 deg C, 1 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 65, # 8 p. 2372 - 2393
反应条件
1H-imidazole in methanol 72 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 35, # 19 p. 3041 - 3044
反应条件
1: 77 percent / pyridine, triethylamine, 4-dimethylaminopyridine / 4 h 2: pyridine, triethylamine, 4-dimethylaminopyridine / 0.5 h 3: pyridine, triethylamine, 4-dimethylaminopyridine / 2 h / Ambient temperature 4: 29percent aq. ammonia, 4-dimethylaminopyridine / pyridine; triethylamine / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1316 - 1319
反应条件
1: pyridine, triethylamine, 4-dimethylaminopyridine / 0.5 h 2: pyridine, triethylamine, 4-dimethylaminopyridine / 2 h / Ambient temperature 3: 29percent aq. ammonia, 4-dimethylaminopyridine / pyridine; triethylamine / 0.5 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1316 - 1319
反应条件
1: tetrazole / acetonitrile 2: pyridine / 8 h View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 51 p. 8971 - 8974
反应条件
1: NaOH / pyridine; ethanol; H2O / 0.25 h 2: 1.) pyridine, 0 deg C, 16 h, 2.) pyridine, CH3OH, 20 deg C, 1 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 65, # 8 p. 2372 - 2393
反应条件
pyridine T=20°C; 2.5 h;
参考文献
EP1253154 A1, ;
Example 2 ;