1-苄基-1,5-二氢-吡咯-2-酮合成路线 (共 23 条)
反应条件
Mo(CHCMe2Ph)lt;N-2,6-(i-Pr)2C6H3gt;lt;OCMe(CF3)2gt;2 in benzene
T=50°C; 2 h;
参考文献
Fu, Gregory C.; Grubbs, Robert H.
Journal of the American Chemical Society, 1992 , vol. 114, # 18 p. 7324 - 7325
反应条件
dihydrogen peroxide in ethyl acetate
T=-5°C; 3.5 h;
参考文献
Mun, JiYoung; Smith, Michael B.
Synthetic Communications, 2007 , vol. 37, # 5 p. 813 - 819
反应条件
(SPY-5-31)-dichloro-(κ2(C,O)-(2-isopropyloxybenzylidene))(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)ruthenium in toluene
T=70°C; 1 h; Inert atmosphere; Catalytic behavior; regioselective reaction;
参考文献
Benedetti, Erica; Lomazzi, Michela; Tibiletti, Francesco; Palmisano, Giovanni; Penoni, Andrea; Goddard, Jean-Philippe; Fensterbank, Louis; Malacria, Max
Synthesis, 2012 , vol. 44, # 22 art. no. 6763, p. 3523 - 3533,11
反应条件
[Cp*Ir(SnCl3)2{SnCl2(H2O)2}]*3H2O; methoxybenzene in 1,2-dichloro-ethane
T=80°C; 20 h; Inert atmosphere;
参考文献
Maity, Arnab Kumar; Roy, Sujit
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2935 - 2941
反应条件
dihydrogen peroxide in ethanol
T=0°C; 0.5 h;
参考文献
Santaniello, Enzo; Casati, Rosangela; Manzocchi, Ada
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2389 - 2392
反应条件
bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; magnesium; tert-butyl alcohol in tetrahydrofuran
T=20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Zheng, Xiao; Dai, Xi-Jie; Yuan, Hong-Qiu; Ye, Chen-Xi; Ma, Jie; Huang, Pei-Qiang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3494 - 3498
Angew. Chem., 2013 , vol. 125, # 12 p. 3578 - 3582,5
反应条件
bis(tricyclohexylphosphine)benzylidene ruthenium(IV) dichloride in dichloromethane
16 h; Heating;
参考文献
Vo-Thanh; Boucard; Sauriat-Dorizon; Guibe
Synlett, 2001 , # 1 p. 37 - 40
反应条件
bis(cyclopentadienyl)titanium dichloride; chloro-trimethyl-silane; magnesium in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Zheng, Xiao; Dai, Xi-Jie; Yuan, Hong-Qiu; Ye, Chen-Xi; Ma, Jie; Huang, Pei-Qiang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 12 p. 3494 - 3498
Angew. Chem., 2013 , vol. 125, # 12 p. 3578 - 3582,5
反应条件
hydrogenchloride in water
T=20°C; 5 h;
参考文献
Xie, Yinjun; Zhao, Yingwei; Qian, Bo; Yang, Lei; Xia, Chungu; Huang, Hanmin
Angewandte Chemie - International Edition, 2011 , vol. 50, # 25 p. 5682 - 5686
反应条件
[Cp*Ir(SnCl3)2{SnCl2(H2O)2}]*3H2O in 1,2-dichloro-ethane
T=80°C; 2 h; Inert atmosphere;
参考文献
Maity, Arnab Kumar; Roy, Sujit
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2935 - 2941