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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
64372-69-6
合成路线
（共 16 条）
64372-69-6
→
反应条件
3258-05-7
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 90 percent / 28percent ammonium hydroxide / 2 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
70421-26-0
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 95 percent / methanol / 6 h / Ambient temperature View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-34-2
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 71 percent / ethanol / 6 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-35-3
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 71 percent / ethanol / 6 h / Heating 3: 87.5 percent / sat. methanolic ammonia / 24 h / 3 °C View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-36-4
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 42 percent / ethanol / 18 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-37-5
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 37.5 percent / ethanol / 18 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-38-6
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 42 percent / ethanol / 20 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-39-7
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 34 percent / ethanol / 20 h / Heating View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-40-0
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 75 percent / sodium / ethanol / 18 h / Heating 3: 0.1 g / ammonium hydroxide / Raney nickel / ethanol / 96 h / 135 °C / steel bomb View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
64372-69-6
→
反应条件
78586-42-2
反应条件
1: 97 percent / thionyl chloride, DMF / CH2Cl2 / 14 h / 60 °C 2: 95.4 percent / ethanol / 18 h / Ambient temperature View Scheme
参考文献
Bhat; Montero; Panzica; Wotring; Townsend
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1165 - 1172
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