N-(2,5-二甲基苯基)肼硫代甲酰胺合成路线 （共 5 条）
反应条件
hydrazine hydrate in ethanol
T=80°C; 1 h;
参考文献
Sriram, Dharmarajan; Yogeeswari, Perumal; Dhakla, Prathiba; Senthilkumar, Palaniappan; Banerjee, Debjani; Manjashetty, Thimmappa H.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 4 p. 1152 - 1154
反应条件
1: With sodium salt of the chloroacetic acid in ethanol
T=20°C; 0.5 h;
2: With hydrazine hydrate in ethanol
T=20°C; 1 h;
参考文献
Liu, Yang; Cui, Kunqiang; Lu, Weiqiang; Luo, Wei; Wang, Jian; Huang, Jin; Guo, Chun
Molecules, 2011 , vol. 16, # 6 p. 4527 - 4538
反应条件
1.1: ammonia / ethanol / 1 h / 20 °C
2.1: sodium salt of the chloroacetic acid / ethanol / 0.5 h / 20 °C
2.2: 1 h / 20 °C
View Scheme
参考文献
Liu, Yang; Cui, Kunqiang; Lu, Weiqiang; Luo, Wei; Wang, Jian; Huang, Jin; Guo, Chun
Molecules, 2011 , vol. 16, # 6 p. 4527 - 4538
反应条件
1: With ammonia in ethanol; water
0.75 h;
2: With sodium carbonate; chloroacetic acid in ethanol; water
3: With hydrazine in ethanol; water
0.75 h; Reflux;
参考文献
Pareek, Alok K.; Joseph; Seth, Daya S.
Oriental Journal of Chemistry, 2010 , vol. 26, # 4 p. 1549 - 1552
参考文献
Nagarajan, K.; Talwalker, P.K.; Kulkarni, C.L.; Venkateswarlu, A.; Prabhu, S.S.; Nayak, G.V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 12 p. 1243 - 1257
