1,3,4,6-四硫并环戊烯-2,5-二酮合成路线 （共 17 条）
反应条件
triethyl phosphite in benzene
byproducts: C8S8O2;
参考文献
Schumaker, Robert R.; Engler, Edward M.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6651 - 6652
Title/Abstract Full Text View citing articles Show Details
Engler, E. M.; Schumaker, R. R.; Kaufman, F. B.
NATO Conf. Ser. VI, 1978 , vol. 1, p. 31 - 34
C.A., 1979 , vol. 91, p. 108434
反应条件
phosphorous acid trimethyl ester in benzene
Heating;
参考文献
Schumaker, Robert R.; Engler, Edward M.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6651 - 6652
反应条件
tetra-(n-butyl)ammonium iodide
1.) DMF, electrochemical reduction: mercury pool, 2.) 0.5 h; Yield given. Multistep reaction;
参考文献
Falsig, Mogens; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 591 - 596
反应条件
Aliquatreg; 336; sodium carbonate in water; benzene
T=40 - 45°C; 2 h;
参考文献
Schumaker, R. R.; Lee, V. Y.; Engler, E. M.
Journal of Organic Chemistry, 1984 , vol. 49, p. 564 - 566
反应条件
sodium methylate
1.) MeOH, RT, 10 min, 2.) MeOH, RT, 3 h; Yield given. Multistep reaction;
参考文献
Mueller, Harald; Ueba, Yoshinobu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 6 p. 1773 - 1777
反应条件
phosphorous acid trimethyl ester in benzene
Heating;
参考文献
Schumaker, Robert R.; Engler, Edward M.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6651 - 6652
反应条件
tetra-(n-butyl)ammonium iodide
1.) DMF, electrochemical reduction: mercury pool, 2.) 0.5 h; Yield given. Multistep reaction;
参考文献
Falsig, Mogens; Lund, Henning
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 8 p. 591 - 596
