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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1,3-二甲基芘
合成路线
（共 25 条）
1059629-90-1
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: KOH / bis-(2-hydroxy-ethyl) ether / 3 h / 180 °C 2: 78 percent / Nafion-H, toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Fujimoto, Masakazu; Nagano, Yoshiaki; Miyazawa, Akira; Tashiro, Masashi
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 321 - 330
77180-48-4
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 25 percent / KOH, NaBH4 / benzene; ethanol / 6 h 2: MCPBA / CHCl3 / 6 h / -5 °C 3: 6.1 percent / 480 °C / 0.8 Torr 4: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
77180-45-1
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 35 percent / KOH, NaBH4 / benzene; ethanol / 6 h 2: 100 percent / MCPBA / CHCl3 / 6 h / -5 °C 3: 6.1 percent / 480 °C / 0.8 Torr 4: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
77180-46-2
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 44 percent / KOH, NaBH4 / benzene; ethanol / 6 h 2: 100 percent / MCPBA / CHCl3 / 6 h / -5 °C 3: 6.1 percent / 480 °C / 0.8 Torr 4: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
77180-50-8
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 41 percent / KOH, NaBH4 / benzene; ethanol / 6 h 2: MCPBA / CHCl3 / 6 h / -5 °C 3: 6.1 percent / 480 °C / 0.8 Torr 4: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
155386-63-3
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: MCPBA / CHCl3 / 6 h / -5 °C 2: 6.1 percent / 480 °C / 0.8 Torr 3: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
155386-66-6
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 100 percent / MCPBA / CHCl3 / 6 h / -5 °C 2: 6.1 percent / 480 °C / 0.8 Torr 3: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
155386-72-4
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: 100 percent / MCPBA / CHCl3 / 6 h / -5 °C 2: 6.1 percent / 480 °C / 0.8 Torr 3: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
155386-74-6
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: MCPBA / CHCl3 / 6 h / -5 °C 2: 6.1 percent / 480 °C / 0.8 Torr 3: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
155386-73-5
→
反应条件
64401-21-4
1,3-二甲基芘
反应条件
1: MCPBA / CHCl3 / 6 h / -5 °C 2: 6.1 percent / 480 °C / 0.8 Torr 3: 78 percent / Nafion-H / toluene / 12 h / Heating View Scheme
参考文献
Yamato, Takehiko; Miyazawa, Akira; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3127 - 3138
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