N-(4-甲氧基苯基)-2-噻吩羧酰胺合成路线 (共 5 条)
反应条件
CuDPP in N,N-dimethyl-formamide
T=60°C; 12 h; Inert atmosphere;
参考文献
Zhang, Zhihui; Yu, Ying; Liebeskind, Lanny S.
Organic Letters, 2008 , vol. 10, # 14 p. 3005 - 3008
反应条件
trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); 1,8-diazabicyclo[5.4.0]undec-7-ene; [(t-Bu)3PH]BF4 in 1,4-dioxane
T=125°C; 3.5 h;
参考文献
Begouin, Agathe; Queiroz, Maria-Joao R. P.
European Journal of Organic Chemistry, 2009 , # 17 p. 2820 - 2827
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane
T=110°C; 1 h;
参考文献
Begouin, Agathe; Queiroz, Maria-Joao R. P.
European Journal of Organic Chemistry, 2009 , # 17 p. 2820 - 2827
反应条件
1: SOCl2 / 0.5 h / Heating
2: triethylamine / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Lee, Chang Kiu; Yu, Ji Sook; Ji, Young Ran
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1219 - 1227
反应条件
triethylamine in dichloromethane
1 h; Heating;
参考文献
Lee, Chang Kiu; Yu, Ji Sook; Ji, Young Ran
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1219 - 1227