1-{2-脱氧-5-O-[(2,3-二甲氧基苯基)(二苯基)甲基]呋喃戊糖基}-5-(1-丙炔-1-基)-2,4(1H,3H)-嘧啶二酮合成路线 （共 4 条）
反应条件
1: NEt3 / tetrahydrofuran
2: NEt3; CuI / Pd(PPh3)4 / acetone
View Scheme
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
反应条件
1: NEt3 / tetrahydrofuran
2: NEt3; CuI / Pd(PPh3)4 / acetone
View Scheme
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
反应条件
copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) in acetone
Sonogashira coupling;
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
反应条件
1: NEt3; CuI / methanol
2: 49 percent / NH3 / methanol; tetrahydrofuran / 22 h / 50 °C
View Scheme
参考文献
Berry, David A.; Jung, Kee-Yong; Wise, Dean S.; Sercel, Anthony D.; Pearson, William H.; Mackie, Hugh; Randolph, John B.; Somers, Robert L.
Tetrahedron Letters, 2004 , vol. 45, # 11 p. 2457 - 2461
