diethyl ether Eintragen einer Loesung des erhaltenen Diazoketons in Dioxan in eine Suspension von Silberoxid in wss. Natriumthiosulfat-Loesung bei 70grad;
参考文献
Litvan; Robinson
Journal of the Chemical Society, 1938 , p. 1997,1999
1: 85 percent / Et3N / CH2Cl2; benzene / 1 h / 20 °C 2: 95 percent Spectr. / CDCl3 / 5 h / 20 °C / Irradiation View Scheme
参考文献
Mantecon, Susana; Vaquero, Juan J.; Alvarez-Builla, Julio; De La Puente, Maria Luz; Espinosa, Juan F.; Ezquerra, Jesus
Organic Letters, 2003 , vol. 5, # 21 p. 3791 - 3794
1: 3-phenyl-propionyl chloride With triethylamine in dichloromethane T=20°C; 16 h; 2: ethylmagnesium bromide in tetrahydrofuran T=0°C; 1 h; 3: With hydrogenchloride in tetrahydrofuran T=0°C; 0.25 h; Further stages.;
参考文献
Hansen, Anne-Lene L.; Murray, Anthony; Tanner, David
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 24 p. 4497 - 4505
