1: With magnesium in tetrahydrofuran T=20°C; 2 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=0°C; 2 h; 3: With ammonia; iodine in tetrahydrofuran; water
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78 - -40°C; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
1: With trimethylsilylazide; boron trifluoride diethyl etherate in dichloromethane T=20°C; 21.5 h; RefluxInert atmosphere; 2: in acetonitrile; mineral oil
参考文献
Hesek, Dusan; Lee, Mijoon; Zhang, Weilie; Noll, Bruce C.; Mobashery, Shahriar
Journal of the American Chemical Society, 2009 , vol. 131, p. 5187 - 5193
