in dichloromethane
Kinetics; byproducts: H2O; to soln. of HCo(CO)4 in CH2Cl2 added Ph3COH in the same solvent under CO at 0 or 20°C in presence of catalytic amts. of HBF4*Et2O, quenched with NH2CH2CH2NH2;
参考文献
Matsui, Yasushi; Orchin, Milton
Journal of Organometallic Chemistry, 1982 , vol. 236, # 3 p. 381 - 384
in methanol; hexane
at -20°C for 20 h in H2 atm. or under N2 or under CO; various yields in various conditions; products were determined colorimetrically using indonaphthol (NH3) and p-(dimethylamino)benzaldehyde (N2H2);
参考文献
Nishihara, Hiroshi; Mori, Takehiko; Tsurita, Yasushi; Nakano, Koji; Saito, Taro; Sasaki, Yukiyoshi
Journal of the American Chemical Society, 1982 , vol. 104, # 16 p. 4367 - 4372
