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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
64567-60-8
合成路线
（共 9 条）
94464-27-4
→
反应条件
64567-60-8
反应条件
hydrogen; acetic acid; palladium on activated charcoal in ethyl acetate T=20°C; 1 h;
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
5840-65-3
→
反应条件
64567-60-8
反应条件
1: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 2: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
90802-45-2
→
反应条件
64567-60-8
反应条件
1: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 2: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
610-35-5
4-羟基邻苯二甲酸
→
反应条件
64567-60-8
反应条件
1: 100 percent / aq. KOH / 12 h / 120 °C 2: 60 percent / 1 h / 200 °C 3: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 4: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
85535-45-1
(S)-5-氨基-2-(Boc-氨基)-5-酮基戊酸
→
反应条件
64567-60-8
反应条件
1: 90 percent / 1,1'-carbonyldiimidazole; 4-dimethylaminopyridine; triethylamine / tetrahydrofuran / 72 h / 20 °C 2: 98 percent / HBr; AcOH / 0.5 h / 20 °C 3: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 4: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
5840-66-4
→
反应条件
64567-60-8
反应条件
1: 60 percent / 1 h / 200 °C 2: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 3: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
31140-42-8
3-N-叔丁氧羰基氨基-2,6-二氧代哌啶
→
反应条件
64567-60-8
反应条件
1: 98 percent / HBr; AcOH / 0.5 h / 20 °C 2: 98 percent / N-ethyl-N'-(3-dimethylaminopropyl)carbodiimide hydrochloride; 1-hydroxybenzotriazole monohydrate; TEA / CH2Cl2 / 72 h / 20 °C 3: 59 percent / H2; acetic acid / Pd/C / ethyl acetate / 1 h / 20 °C View Scheme
参考文献
Nakamura, Takanori; Noguchi, Tomomi; Kobayashi, Hisayoshi; Miyachi, Hiroyuki; Hashimoto, Yuichi
Chemical and Pharmaceutical Bulletin, 2006 , vol. 54, # 12 p. 1709 - 1714
27550-63-6
→
反应条件
64567-60-8
+
857184-58-8
反应条件
in acetic acid 52 h; RefluxInert atmosphere;
参考文献
Luo, Weiming; Yu, Qian-Sheng; Tweedie, David; Deschamps, Jeffery; Parrish, Damon; Holloway, Harold W.; Li, Yazhou; Brossi, Arnold; Greig, Nigel H.
Synthesis, 2008 , # 21 art. no. M02108SS, p. 3415 - 3422
27550-59-0
4-羟基苯酐
→
反应条件
64567-60-8
反应条件
in tetrahydrofuran; acetic acid 4.5 h; RefluxInert atmosphere;
参考文献
Luo, Weiming; Yu, Qian-Sheng; Tweedie, David; Deschamps, Jeffery; Parrish, Damon; Holloway, Harold W.; Li, Yazhou; Brossi, Arnold; Greig, Nigel H.
Synthesis, 2008 , # 21 art. no. M02108SS, p. 3415 - 3422
