2-羟基-1-(4-硝基苯基)-1-乙酮合成路线 （共 20 条）
反应条件
toluene-4-sulfonic acid in tetrahydrofuran; water 4.5 h; Reflux;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., , vol. 124, # 50 p. 12738 - 12742,5
反应条件
in dichloromethane 17 h; Ambient temperature;
参考文献
Synthesis, , # 12 p. 980 - 981
反应条件
perchloric acid; water T=20°C; other reagent, kinetic solvent isotope effect; Rate constant;
参考文献
Doklady Chemistry, , vol. 291, p. 477 - 480
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 291, # 4 p. 874 - 877
反应条件
1: α-hydroxy-p-nitroacetophenone With triethylamine in dichloromethane 24 h; Heating; 2: ethanethioamide With potassium carbonate in acetonitrile 10 h; Heating; Further stages.;
参考文献
Liu, Xiao-Ling; Wang, Qiu-Ying; Sheng, Shou-Ri; Xu, Chen; Cai, Ming-Zhong
Synthetic Communications, 2008 , vol. 38, # 19 p. 3338 - 3345
反应条件
18-crown-6 ether; oxygen; potassium carbonate in tetrahydrofuran; water T=70°C; P=760.051 Torr; 24 h;
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
FPIFA in water; benzene Mechanism;
参考文献
Moriarty, Robert M.; Prakash, Indra; Penmasta, Raju
Journal of the Chemical Society, Chemical Communications, 1987 , # 3 p. 202 - 203
反应条件
18-crown-6 ether; oxygen; potassium carbonate in water
T=80°C; P=760.051 Torr; 10 h;
参考文献
Liu, Hui; Dong, Chao; Zhang, Zeguang; Wu, Peiyu; Jiang, Xuefeng
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12570 - 12574
Angew. Chem., 2012 , vol. 124, # 50 p. 12738 - 12742,5
反应条件
diethylamine in methanol
T=20°C; 1 h;
参考文献
Hirst, Gavin C.; Arnold, Lee D.; Burchat, Andrew; Wishart, Neil; Calderwood, David; Wada, Carol K.; Michaelides, Michael R.; Ji, Zhiqin; Muckey, Melanie
Patent: US2003/225098 A1, 2003 ;
Location in patent: Page 32 ;
US 20030225098 A1
反应条件
in methanol; ethyl acetate
参考文献
Hirst, Gavin C.; Arnold, Lee D.; Burchat, Andrew; Wishart, Neil; Wada, Carol K.; Michaelides, Michael R.; Ji, Zhiqin; Muckey, Melanie
Patent: US2003/199525 A1, 2003 ;
反应条件
in acetonitrile
2 h; Heating;
参考文献
Peach, Philip; Cross, David J.; Kenny, Jennifer A.; Mann, Inderjit; Houson, Ian; Campbell, Lynne; Walsgrove, Tim; Wills, Martin
Tetrahedron, 2006 , vol. 62, # 8 p. 1864 - 1876
