2-羟基-4,4,6,6-四甲基环己-2-烯-1-酮合成路线 （共 16 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; potassium tert-butylate; oxygen in tert-butyl alcohol
参考文献
Hanna,R.; Ourisson,G.
Bulletin de la Societe Chimique de France, 1967 , p. 3742 - 3747
反应条件
1: SeO2 / dioxane
2: aq. KOH / diethyl ether
View Scheme
参考文献
Korobitsyna,I.K.; Nikolaev,V.A.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 1245 - 1251
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 1244 - 1251
反应条件
1: 1) Mg, 2) Cu(I)
2: 84.6 percent / Br2 / acetic acid
3: 84 percent / KOH
View Scheme
参考文献
Gill, G. Bryon; Idris, Muhammad S. Hj.; Kirollos, Kirollos S.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2355 - 2366
反应条件
potassium hydroxide in diethyl ether
参考文献
Korobitsyna,I.K.; Nikolaev,V.A.
Journal of Organic Chemistry USSR (English Translation), 1976 , vol. 12, p. 1245 - 1251
Zhurnal Organicheskoi Khimii, 1976 , vol. 12, p. 1244 - 1251
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
1: 45 percent / selenium dioxide / methanol / 168 h / Heating
2: 35 percent / sodium periodate / methanol / 0.75 h
View Scheme
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
