2-羟基-4,4,6,6-四甲基环己-2-烯-1-酮合成路线 (共 16 条)
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
selenium(IV) oxide in methanol
168 h; Heating; Further byproducts given. Title compound not separated from byproducts;
参考文献
Laitalainen, Tarja; Simonen, Tapio; Kivekaes, Raikko; Klinga, Martti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 333 - 340
反应条件
1: 70 percent / Br2 / acetic acid
2: 62 percent / 1M NaOH / 110 °C
3: 57 percent / I2, KI
4: 90 percent / P2O5 / neat (no solvent) / 38 °C / 10 Torr
View Scheme
参考文献
Hesse,G.; Beyer,P.
Justus Liebigs Annalen der Chemie, 1971 , vol. 747, p. 84 - 97