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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
64648-12-0
合成路线
（共 5 条）
64648-11-9
→
反应条件
64648-12-0
反应条件
dihydrogen peroxide in acetic acid 20 h; Ambient temperature;
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
150-60-7
二苄基二硫
→
反应条件
64648-12-0
反应条件
1: 69 percent / MCPBA / CH2Cl2 / 5 h / 0 °C 2: 24 percent / acetic acid / 1 h / 60 °C 3: 74 percent / 30percent H2O2 / acetic acid / 20 h / Ambient temperature View Scheme
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
16302-98-0
→
反应条件
64648-12-0
反应条件
1: 24 percent / acetic acid / 1 h / 60 °C 2: 74 percent / 30percent H2O2 / acetic acid / 20 h / Ambient temperature View Scheme
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
41719-05-5
→
反应条件
64648-12-0
反应条件
1: 64 percent / triethyl amine / diethyl ether / 0.33 h / -20 °C 2: 24 percent / acetic acid / 1 h / 60 °C 3: 74 percent / 30percent H2O2 / acetic acid / 20 h / Ambient temperature View Scheme
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
100-53-8
苄硫醇
→
反应条件
64648-12-0
反应条件
1: 64 percent / triethyl amine / diethyl ether / 0.33 h / -20 °C 2: 24 percent / acetic acid / 1 h / 60 °C 3: 74 percent / 30percent H2O2 / acetic acid / 20 h / Ambient temperature View Scheme
参考文献
Furukawa, Naomichi; Morishita, Tsuyoshi; Akasaka, Takeshi; Oae, Shigeru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 432 - 440
