3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 合成路线 （共 69 条）
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
hydrogenchloride; formic acid; oxygen; copper; zinc in water T=80°C; 2 h; various solvents, water concentration; Product distribution;
参考文献
Blancou,H.; Benefice,S.
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
1: With sulfuric acid; sulfur trioxide in water T=30°C; 1.66 h; 2: With sodium sulfite; water T=0 - 80°C; 2 h; Product distribution / selectivity;
参考文献
DAIKIN INDUSTRIES, LTD.
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
(10H)-phenothiazine in tert-butyl alcohol T=130 - 170°C; 6 - 9 h;
参考文献
EP1486482 A1, ;
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
lithium triethylborohydride in tetrahydrofuran T=20°C; 2 h;
参考文献
Eames, Jason; Khanom, Hasina
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
pyrrolidin-2-one T=140°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 7 p. 2059 - 2071
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
1: With benzo[1,3,2]dioxaborole; [Rh[(R)-BINAP](COD)]BF4 in tetrahydrofuran T=0°C; 1 h; 2: With sodium hydroxide; dihydrogen peroxide in ethanol Further stages. Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 4 p. 464 - 465
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
1: With Wilkinson's catalyst in tetrahydrofuran T=20°C; 2.5 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 1, # 9 p. 1399 - 1402
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇 +
反应条件
1: With Wilkinson's catalyst in tetrahydrofuran T=20°C; 0.5 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 1, # 9 p. 1399 - 1402
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
lithium triethylborohydride in tetrahydrofuran T=20°C; 2 h;
参考文献
Eames, Jason; Khanom, Hasina
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反应条件
647-42-7 3,3,4,4,5,5,6,6,7,7,8,8,8-十三氟-1-辛醇
反应条件
lithium triethylborohydride in tetrahydrofuran T=20°C; 2 h;
参考文献
Eames, Jason; Khanom, Hasina
